Direct synthesis of mesoporous aluminosilicates from Indonesian kaolin clay without calcination

Imroatul Qoniah; Didik Prasetyoko; Hasliza Bahruji; Sugeng Triwahyono; Aishah Abdul Jalil; Hartati; Tri Esti Purbaningtias

doi:10.1016/j.clay.2015.10.007

Direct synthesis of mesoporous aluminosilicates from Indonesian kaolin clay without calcination

Imroatul Qoniah
, Didik Prasetyoko^*
, Hasliza Bahruji
, Sugeng Triwahyono
, Aishah Abdul Jalil
, Suprapto
, Hartati
, Tri Esti Purbaningtias

^*Corresponding author for this work

Department of Environmental Engineering
Islamic University of Jl
Chemistry Department
Institut Teknologi Sepuluh Nopember
Cardiff Catalysis Institute
Cardiff University
Ibnu Sina Institute for Fundamental Science Studies
Universiti Teknologi Malaysia
Department of Chemistry
Universitas Airlangga
Diploma of Analytical Chemistry
Islamic University of Jl. Kaliurang Km. 14.5

Research output: Contribution to journal › Article › peer-review

43 Citations (Scopus)

Abstract

The transformation of kaolin to amorphous mesoporous aluminosilicate was investigated in this study. We demonstrated the use of koalin as silica and alumina sources without prior pretreatment. Two steps synthesis method were carried out; hydrothermal reaction at 80. °C, followed by addition of mesoporogen cetyltrimethylammonium bromide (CTABr) surfactant. We observed that prolonging the synthesis period improves the surface area of the aluminosilicate with enhances mesopore volume and surface acidity.

Original language	English
Pages (from-to)	290-294
Number of pages	5
Journal	Applied Clay Science
Volume	118
DOIs	https://doi.org/10.1016/j.clay.2015.10.007
Publication status	Published - 1 Dec 2015

Keywords

Aluminosilicates based-materials
Kaolin
Mesoporous
Surface acidity

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10.1016/j.clay.2015.10.007

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title = "Direct synthesis of mesoporous aluminosilicates from Indonesian kaolin clay without calcination",

abstract = "The transformation of kaolin to amorphous mesoporous aluminosilicate was investigated in this study. We demonstrated the use of koalin as silica and alumina sources without prior pretreatment. Two steps synthesis method were carried out; hydrothermal reaction at 80. °C, followed by addition of mesoporogen cetyltrimethylammonium bromide (CTABr) surfactant. We observed that prolonging the synthesis period improves the surface area of the aluminosilicate with enhances mesopore volume and surface acidity.",

keywords = "Aluminosilicates based-materials, Kaolin, Mesoporous, Surface acidity",

author = "Imroatul Qoniah and Didik Prasetyoko and Hasliza Bahruji and Sugeng Triwahyono and Jalil, \{Aishah Abdul\} and Suprapto and Hartati and Purbaningtias, \{Tri Esti\}",

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doi = "10.1016/j.clay.2015.10.007",

language = "English",

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T1 - Direct synthesis of mesoporous aluminosilicates from Indonesian kaolin clay without calcination

AU - Qoniah, Imroatul

AU - Prasetyoko, Didik

AU - Bahruji, Hasliza

AU - Triwahyono, Sugeng

AU - Jalil, Aishah Abdul

AU - Suprapto,

AU - Hartati,

AU - Purbaningtias, Tri Esti

PY - 2015/12/1

Y1 - 2015/12/1

N2 - The transformation of kaolin to amorphous mesoporous aluminosilicate was investigated in this study. We demonstrated the use of koalin as silica and alumina sources without prior pretreatment. Two steps synthesis method were carried out; hydrothermal reaction at 80. °C, followed by addition of mesoporogen cetyltrimethylammonium bromide (CTABr) surfactant. We observed that prolonging the synthesis period improves the surface area of the aluminosilicate with enhances mesopore volume and surface acidity.

AB - The transformation of kaolin to amorphous mesoporous aluminosilicate was investigated in this study. We demonstrated the use of koalin as silica and alumina sources without prior pretreatment. Two steps synthesis method were carried out; hydrothermal reaction at 80. °C, followed by addition of mesoporogen cetyltrimethylammonium bromide (CTABr) surfactant. We observed that prolonging the synthesis period improves the surface area of the aluminosilicate with enhances mesopore volume and surface acidity.

KW - Aluminosilicates based-materials

KW - Kaolin

KW - Mesoporous

KW - Surface acidity

UR - https://www.scopus.com/pages/publications/84957725802

U2 - 10.1016/j.clay.2015.10.007

DO - 10.1016/j.clay.2015.10.007

M3 - Article

AN - SCOPUS:84957725802

SN - 0169-1317

VL - 118

SP - 290

EP - 294

JO - Applied Clay Science

JF - Applied Clay Science

ER -

Direct synthesis of mesoporous aluminosilicates from Indonesian kaolin clay without calcination

Abstract

Keywords

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