Effect of addition octadecyltrimethoxysilane (OTMS) on morphology ZSM-5-TiO2 composite

A. Iryani; R. Kurniawati; D. Hartanto; M. Santoso; H. Nur

doi:10.1063/5.0001723

Effect of addition octadecyltrimethoxysilane (OTMS) on morphology ZSM-5-TiO₂ composite

A. Iryani, R. Kurniawati, D. Hartanto^*, M. Santoso, H. Nur

^*Corresponding author for this work

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

2 Citations (Scopus)

Abstract

ZSM-5-TiO₂ composites are usually used as adsorbents as well as photocatalyst in waste treatment. However, these composites are less effective insoluble waste treatment, so it needs to modify by adding organic substances that can react with the waste. In this study, Octadecyltrimethoxysilane (OTMS) was added to the surface of the ZSM-5-TiO₂ composite. The effect of addition OTMS on morphology ZSM-5-TiO₂ composite was studied. ZSM-5-TiO₂-OTMS composite was characterized by X-Ray Diffraction (XRD), Fourier Transformation Infrared Spectroscopy (FTIR), and Energy Dispersive X-ray Scanning Electron Microscopy (SEM-EDX). ZSM-5-TiO₂-OTMS shows a carbon-related peak at 2900 and 1470 cm^-1 that can be ascribed as C-H stretching and C-O stretching vibration respectively from FTIR spectra. ZSM-5-TiO₂-OTMS composite retains the hexagonal shape surrounded by round-shaped. The addition of OTMS affects the morphology of the ZSM-5-TiO₂ composite. The more OTMS is added, the morphology of the ZSM-5-TiO₂-OTMS composite to be more irregular than composite ZSM-5-TiO₂. It also affects the amount of carbon content that is distributed on the surface of the ZSM-5-TiO₂ composite. This provides information material that can be used in synthesize catalysts in the insoluble waste treatment.

Original language	English
Title of host publication	8th International Conference of the Indonesian Chemical Society, ICICS 2019
Editors	Mohamad Rafi, Rudi Heryanto, Wulan Tri Wahyuni
Publisher	American Institute of Physics Inc.
ISBN (Electronic)	9780735420021
DOIs	https://doi.org/10.1063/5.0001723
Publication status	Published - 4 Jun 2020
Event	8th International Conference of the Indonesian Chemical Society 2019, ICICS 2019 - Bogor, Indonesia Duration: 6 Aug 2019 → 7 Aug 2019

Publication series

Name	AIP Conference Proceedings
Volume	2243
ISSN (Print)	0094-243X
ISSN (Electronic)	1551-7616

Conference

Conference	8th International Conference of the Indonesian Chemical Society 2019, ICICS 2019
Country/Territory	Indonesia
City	Bogor
Period	6/08/19 → 7/08/19

Access to Document

10.1063/5.0001723

Cite this

Iryani, A., Kurniawati, R., Hartanto, D., Santoso, M., & Nur, H. (2020). Effect of addition octadecyltrimethoxysilane (OTMS) on morphology ZSM-5-TiO₂ composite. In M. Rafi, R. Heryanto, & W. T. Wahyuni (Eds.), 8th International Conference of the Indonesian Chemical Society, ICICS 2019 Article 020011 (AIP Conference Proceedings; Vol. 2243). American Institute of Physics Inc.. https://doi.org/10.1063/5.0001723

@inproceedings{36b8d059d9bd42568c2106ce107dd725,

title = "Effect of addition octadecyltrimethoxysilane (OTMS) on morphology ZSM-5-TiO2 composite",

abstract = "ZSM-5-TiO2 composites are usually used as adsorbents as well as photocatalyst in waste treatment. However, these composites are less effective insoluble waste treatment, so it needs to modify by adding organic substances that can react with the waste. In this study, Octadecyltrimethoxysilane (OTMS) was added to the surface of the ZSM-5-TiO2 composite. The effect of addition OTMS on morphology ZSM-5-TiO2 composite was studied. ZSM-5-TiO2-OTMS composite was characterized by X-Ray Diffraction (XRD), Fourier Transformation Infrared Spectroscopy (FTIR), and Energy Dispersive X-ray Scanning Electron Microscopy (SEM-EDX). ZSM-5-TiO2-OTMS shows a carbon-related peak at 2900 and 1470 cm-1 that can be ascribed as C-H stretching and C-O stretching vibration respectively from FTIR spectra. ZSM-5-TiO2-OTMS composite retains the hexagonal shape surrounded by round-shaped. The addition of OTMS affects the morphology of the ZSM-5-TiO2 composite. The more OTMS is added, the morphology of the ZSM-5-TiO2-OTMS composite to be more irregular than composite ZSM-5-TiO2. It also affects the amount of carbon content that is distributed on the surface of the ZSM-5-TiO2 composite. This provides information material that can be used in synthesize catalysts in the insoluble waste treatment.",

author = "A. Iryani and R. Kurniawati and D. Hartanto and M. Santoso and H. Nur",

note = "Publisher Copyright: {\textcopyright} 2020 Author(s).; 8th International Conference of the Indonesian Chemical Society 2019, ICICS 2019 ; Conference date: 06-08-2019 Through 07-08-2019",

year = "2020",

month = jun,

day = "4",

doi = "10.1063/5.0001723",

language = "English",

series = "AIP Conference Proceedings",

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Iryani, A, Kurniawati, R, Hartanto, D , Santoso, M & Nur, H 2020, Effect of addition octadecyltrimethoxysilane (OTMS) on morphology ZSM-5-TiO₂ composite. in M Rafi, R Heryanto & WT Wahyuni (eds), 8th International Conference of the Indonesian Chemical Society, ICICS 2019., 020011, AIP Conference Proceedings, vol. 2243, American Institute of Physics Inc., 8th International Conference of the Indonesian Chemical Society 2019, ICICS 2019, Bogor, Indonesia, 6/08/19. https://doi.org/10.1063/5.0001723

Effect of addition octadecyltrimethoxysilane (OTMS) on morphology ZSM-5-TiO₂ composite. / Iryani, A.; Kurniawati, R.; Hartanto, D. et al.
8th International Conference of the Indonesian Chemical Society, ICICS 2019. ed. / Mohamad Rafi; Rudi Heryanto; Wulan Tri Wahyuni. American Institute of Physics Inc., 2020. 020011 (AIP Conference Proceedings; Vol. 2243).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

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AU - Kurniawati, R.

AU - Hartanto, D.

AU - Santoso, M.

AU - Nur, H.

PY - 2020/6/4

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N2 - ZSM-5-TiO2 composites are usually used as adsorbents as well as photocatalyst in waste treatment. However, these composites are less effective insoluble waste treatment, so it needs to modify by adding organic substances that can react with the waste. In this study, Octadecyltrimethoxysilane (OTMS) was added to the surface of the ZSM-5-TiO2 composite. The effect of addition OTMS on morphology ZSM-5-TiO2 composite was studied. ZSM-5-TiO2-OTMS composite was characterized by X-Ray Diffraction (XRD), Fourier Transformation Infrared Spectroscopy (FTIR), and Energy Dispersive X-ray Scanning Electron Microscopy (SEM-EDX). ZSM-5-TiO2-OTMS shows a carbon-related peak at 2900 and 1470 cm-1 that can be ascribed as C-H stretching and C-O stretching vibration respectively from FTIR spectra. ZSM-5-TiO2-OTMS composite retains the hexagonal shape surrounded by round-shaped. The addition of OTMS affects the morphology of the ZSM-5-TiO2 composite. The more OTMS is added, the morphology of the ZSM-5-TiO2-OTMS composite to be more irregular than composite ZSM-5-TiO2. It also affects the amount of carbon content that is distributed on the surface of the ZSM-5-TiO2 composite. This provides information material that can be used in synthesize catalysts in the insoluble waste treatment.

AB - ZSM-5-TiO2 composites are usually used as adsorbents as well as photocatalyst in waste treatment. However, these composites are less effective insoluble waste treatment, so it needs to modify by adding organic substances that can react with the waste. In this study, Octadecyltrimethoxysilane (OTMS) was added to the surface of the ZSM-5-TiO2 composite. The effect of addition OTMS on morphology ZSM-5-TiO2 composite was studied. ZSM-5-TiO2-OTMS composite was characterized by X-Ray Diffraction (XRD), Fourier Transformation Infrared Spectroscopy (FTIR), and Energy Dispersive X-ray Scanning Electron Microscopy (SEM-EDX). ZSM-5-TiO2-OTMS shows a carbon-related peak at 2900 and 1470 cm-1 that can be ascribed as C-H stretching and C-O stretching vibration respectively from FTIR spectra. ZSM-5-TiO2-OTMS composite retains the hexagonal shape surrounded by round-shaped. The addition of OTMS affects the morphology of the ZSM-5-TiO2 composite. The more OTMS is added, the morphology of the ZSM-5-TiO2-OTMS composite to be more irregular than composite ZSM-5-TiO2. It also affects the amount of carbon content that is distributed on the surface of the ZSM-5-TiO2 composite. This provides information material that can be used in synthesize catalysts in the insoluble waste treatment.

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