Electrical characteristics of natural ironstone-derived LiFe0.99Cu0.01PO4and LiFe0.98Cu0.02PO4powders

A. Firdausi; C. Latif; Nihlatunnur; B. Prihandoko; M. Zainuri; S. Pratapa

doi:10.1063/5.0015421

Electrical characteristics of natural ironstone-derived LiFe_0.99Cu_0.01PO₄and LiFe_0.98Cu_0.02PO₄powders

A. Firdausi, C. Latif, Nihlatunnur, B. Prihandoko, M. Zainuri, S. Pratapa^*

^*Corresponding author for this work

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

1 Citation (Scopus)

Abstract

Syntheses of LiFe1-xCuxPO4 (x = 1 and 2 at. %) were successfully carried out using the dissolution method. The source of Fe used was the ironstone from South Kalimantan, and the sources of other components were commercial products. The ironstone was treated using the dissolution method with drying and calcination temperatures of 350°C for 2 hours and 700°C for 10 hours in the N2 atmosphere, respectively. The samples were characterized using X-ray diffractometer (XRD) and scanning electron microscope (SEM), while the electrochemical performances were examined through the charge/discharge (CD) and the cyclic voltammetry (CV) measurements. XRD patterns showed that only LiFePO4 olivine was identified with successful Cu ions substitution. The specific capacities of the LiFe0.99Cu0.01PO4 and LiFe0.98Cu0.02PO4 powders were 5.2 and 14.5 mAh/g, respectively. The sample would be a potential material for lithium battery applications when a conductive layer such as carbon is introduced.

Original language	English
Title of host publication	Proceedings of the 5th International Symposium on Frontier of Applied Physics, ISFAP 2019
Editors	Muhandis Shiddiq, Andri Hardiansyah, Witha Berlian Kesuma Putri, Yuliati Herbani, Edi Kurniawan, Deni Khaerudini, Ahmad Nugraha, Syuhada Syuhada, Hamzah Fauzi, Abdulloh Rifai, Edi Suprayoga, Anggito Tetuko, Toto Sudiro
Publisher	American Institute of Physics Inc.
ISBN (Electronic)	9780735420168
DOIs	https://doi.org/10.1063/5.0015421
Publication status	Published - 3 Sept 2020
Event	5th International Symposium on Frontier of Applied Physics, ISFAP 2019 - Tangerang Selatan, Indonesia Duration: 23 Oct 2019 → 24 Oct 2019

Publication series

Name	AIP Conference Proceedings
Volume	2256
ISSN (Print)	0094-243X
ISSN (Electronic)	1551-7616

Conference

Conference	5th International Symposium on Frontier of Applied Physics, ISFAP 2019
Country/Territory	Indonesia
City	Tangerang Selatan
Period	23/10/19 → 24/10/19

Access to Document

10.1063/5.0015421

Cite this

Firdausi, A., Latif, C., Nihlatunnur, Prihandoko, B., Zainuri, M., & Pratapa, S. (2020). Electrical characteristics of natural ironstone-derived LiFe_0.99Cu_0.01PO₄and LiFe_0.98Cu_0.02PO₄powders. In M. Shiddiq, A. Hardiansyah, W. B. K. Putri, Y. Herbani, E. Kurniawan, D. Khaerudini, A. Nugraha, S. Syuhada, H. Fauzi, A. Rifai, E. Suprayoga, A. Tetuko, & T. Sudiro (Eds.), Proceedings of the 5th International Symposium on Frontier of Applied Physics, ISFAP 2019 Article 030005 (AIP Conference Proceedings; Vol. 2256). American Institute of Physics Inc.. https://doi.org/10.1063/5.0015421

Firdausi, A. ; Latif, C. ; Nihlatunnur et al. / Electrical characteristics of natural ironstone-derived LiFe_0.99Cu_0.01PO₄and LiFe_0.98Cu_0.02PO₄powders. Proceedings of the 5th International Symposium on Frontier of Applied Physics, ISFAP 2019. editor / Muhandis Shiddiq ; Andri Hardiansyah ; Witha Berlian Kesuma Putri ; Yuliati Herbani ; Edi Kurniawan ; Deni Khaerudini ; Ahmad Nugraha ; Syuhada Syuhada ; Hamzah Fauzi ; Abdulloh Rifai ; Edi Suprayoga ; Anggito Tetuko ; Toto Sudiro. American Institute of Physics Inc., 2020. (AIP Conference Proceedings).

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title = "Electrical characteristics of natural ironstone-derived LiFe0.99Cu0.01PO4and LiFe0.98Cu0.02PO4powders",

abstract = "Syntheses of LiFe1-xCuxPO4 (x = 1 and 2 at. %) were successfully carried out using the dissolution method. The source of Fe used was the ironstone from South Kalimantan, and the sources of other components were commercial products. The ironstone was treated using the dissolution method with drying and calcination temperatures of 350°C for 2 hours and 700°C for 10 hours in the N2 atmosphere, respectively. The samples were characterized using X-ray diffractometer (XRD) and scanning electron microscope (SEM), while the electrochemical performances were examined through the charge/discharge (CD) and the cyclic voltammetry (CV) measurements. XRD patterns showed that only LiFePO4 olivine was identified with successful Cu ions substitution. The specific capacities of the LiFe0.99Cu0.01PO4 and LiFe0.98Cu0.02PO4 powders were 5.2 and 14.5 mAh/g, respectively. The sample would be a potential material for lithium battery applications when a conductive layer such as carbon is introduced.",

author = "A. Firdausi and C. Latif and Nihlatunnur and B. Prihandoko and M. Zainuri and S. Pratapa",

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Firdausi, A, Latif, C, Nihlatunnur, Prihandoko, B, Zainuri, M & Pratapa, S 2020, Electrical characteristics of natural ironstone-derived LiFe_0.99Cu_0.01PO₄and LiFe_0.98Cu_0.02PO₄powders. in M Shiddiq, A Hardiansyah, WBK Putri, Y Herbani, E Kurniawan, D Khaerudini, A Nugraha, S Syuhada, H Fauzi, A Rifai, E Suprayoga, A Tetuko & T Sudiro (eds), Proceedings of the 5th International Symposium on Frontier of Applied Physics, ISFAP 2019., 030005, AIP Conference Proceedings, vol. 2256, American Institute of Physics Inc., 5th International Symposium on Frontier of Applied Physics, ISFAP 2019, Tangerang Selatan, Indonesia, 23/10/19. https://doi.org/10.1063/5.0015421

Electrical characteristics of natural ironstone-derived LiFe_0.99Cu_0.01PO₄and LiFe_0.98Cu_0.02PO₄powders. / Firdausi, A.; Latif, C.; Nihlatunnur et al.
Proceedings of the 5th International Symposium on Frontier of Applied Physics, ISFAP 2019. ed. / Muhandis Shiddiq; Andri Hardiansyah; Witha Berlian Kesuma Putri; Yuliati Herbani; Edi Kurniawan; Deni Khaerudini; Ahmad Nugraha; Syuhada Syuhada; Hamzah Fauzi; Abdulloh Rifai; Edi Suprayoga; Anggito Tetuko; Toto Sudiro. American Institute of Physics Inc., 2020. 030005 (AIP Conference Proceedings; Vol. 2256).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

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T1 - Electrical characteristics of natural ironstone-derived LiFe0.99Cu0.01PO4and LiFe0.98Cu0.02PO4powders

AU - Firdausi, A.

AU - Latif, C.

AU - Nihlatunnur,

AU - Prihandoko, B.

AU - Zainuri, M.

AU - Pratapa, S.

PY - 2020/9/3

Y1 - 2020/9/3

N2 - Syntheses of LiFe1-xCuxPO4 (x = 1 and 2 at. %) were successfully carried out using the dissolution method. The source of Fe used was the ironstone from South Kalimantan, and the sources of other components were commercial products. The ironstone was treated using the dissolution method with drying and calcination temperatures of 350°C for 2 hours and 700°C for 10 hours in the N2 atmosphere, respectively. The samples were characterized using X-ray diffractometer (XRD) and scanning electron microscope (SEM), while the electrochemical performances were examined through the charge/discharge (CD) and the cyclic voltammetry (CV) measurements. XRD patterns showed that only LiFePO4 olivine was identified with successful Cu ions substitution. The specific capacities of the LiFe0.99Cu0.01PO4 and LiFe0.98Cu0.02PO4 powders were 5.2 and 14.5 mAh/g, respectively. The sample would be a potential material for lithium battery applications when a conductive layer such as carbon is introduced.

AB - Syntheses of LiFe1-xCuxPO4 (x = 1 and 2 at. %) were successfully carried out using the dissolution method. The source of Fe used was the ironstone from South Kalimantan, and the sources of other components were commercial products. The ironstone was treated using the dissolution method with drying and calcination temperatures of 350°C for 2 hours and 700°C for 10 hours in the N2 atmosphere, respectively. The samples were characterized using X-ray diffractometer (XRD) and scanning electron microscope (SEM), while the electrochemical performances were examined through the charge/discharge (CD) and the cyclic voltammetry (CV) measurements. XRD patterns showed that only LiFePO4 olivine was identified with successful Cu ions substitution. The specific capacities of the LiFe0.99Cu0.01PO4 and LiFe0.98Cu0.02PO4 powders were 5.2 and 14.5 mAh/g, respectively. The sample would be a potential material for lithium battery applications when a conductive layer such as carbon is introduced.

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U2 - 10.1063/5.0015421

DO - 10.1063/5.0015421

M3 - Conference contribution

AN - SCOPUS:85091930398

T3 - AIP Conference Proceedings

BT - Proceedings of the 5th International Symposium on Frontier of Applied Physics, ISFAP 2019

A2 - Shiddiq, Muhandis

A2 - Hardiansyah, Andri

A2 - Putri, Witha Berlian Kesuma

A2 - Herbani, Yuliati

A2 - Kurniawan, Edi

A2 - Khaerudini, Deni

A2 - Nugraha, Ahmad

A2 - Syuhada, Syuhada

A2 - Fauzi, Hamzah

A2 - Rifai, Abdulloh

A2 - Suprayoga, Edi

A2 - Tetuko, Anggito

A2 - Sudiro, Toto

PB - American Institute of Physics Inc.

T2 - 5th International Symposium on Frontier of Applied Physics, ISFAP 2019

Y2 - 23 October 2019 through 24 October 2019

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Firdausi A, Latif C, Nihlatunnur, Prihandoko B, Zainuri M , Pratapa S. Electrical characteristics of natural ironstone-derived LiFe_0.99Cu_0.01PO₄and LiFe_0.98Cu_0.02PO₄powders. In Shiddiq M, Hardiansyah A, Putri WBK, Herbani Y, Kurniawan E, Khaerudini D, Nugraha A, Syuhada S, Fauzi H, Rifai A, Suprayoga E, Tetuko A, Sudiro T, editors, Proceedings of the 5th International Symposium on Frontier of Applied Physics, ISFAP 2019. American Institute of Physics Inc. 2020. 030005. (AIP Conference Proceedings). doi: 10.1063/5.0015421