TY - GEN
T1 - Esterification of glycerol monooleate from glycerol and oleic acid using microwave heating
AU - Qadariyah, Lailatul
AU - Fadilah, Asri Nur
AU - Vincentius, Vincentius
N1 - Publisher Copyright:
© 2023 Author(s).
PY - 2023/2/28
Y1 - 2023/2/28
N2 - Glycerol Monooleate is the non-ionic surfactant that can be produced by the esterification reaction of oleic acid and glycerol. The purpose of this research was to produce Glycerol monooleate using H-ZSM-5 catalyst and microwave as a heat source, and to study all the effect of reaction ratio, reaction time, amount of catalyst and operating temperature. The use of microwave as a heat source serves to increase the effectiveness and efficiency of the esterification process so that the required processing time is faster. The esterification process is carried out using microwave power of 300 watt. Based on the results of the study, the optimum conditions were obtained at a ratio of 2:1 reactant, 1% catalyst weight, reaction time of 50 minutes, and reaction temperature of 160°C with a yield value of 92.02%. So, it can be concluded that the use of a microwave can increase the processing time 40 minutes faster than conventional heaters.
AB - Glycerol Monooleate is the non-ionic surfactant that can be produced by the esterification reaction of oleic acid and glycerol. The purpose of this research was to produce Glycerol monooleate using H-ZSM-5 catalyst and microwave as a heat source, and to study all the effect of reaction ratio, reaction time, amount of catalyst and operating temperature. The use of microwave as a heat source serves to increase the effectiveness and efficiency of the esterification process so that the required processing time is faster. The esterification process is carried out using microwave power of 300 watt. Based on the results of the study, the optimum conditions were obtained at a ratio of 2:1 reactant, 1% catalyst weight, reaction time of 50 minutes, and reaction temperature of 160°C with a yield value of 92.02%. So, it can be concluded that the use of a microwave can increase the processing time 40 minutes faster than conventional heaters.
UR - http://www.scopus.com/inward/record.url?scp=85149996809&partnerID=8YFLogxK
U2 - 10.1063/5.0112813
DO - 10.1063/5.0112813
M3 - Conference contribution
AN - SCOPUS:85149996809
T3 - AIP Conference Proceedings
BT - 2nd International Symposium of Indonesian Chemical Engineering 2021
A2 - Purbasari, Aprilina
A2 - Ariyanti, Dessy
A2 - Suherman, null
A2 - Kumoro, Andri Cahyo
A2 - Kusworo, Tutuk Djoko
A2 - Djaeni, Mohamad
PB - American Institute of Physics Inc.
T2 - 2nd International Symposium of Indonesian Chemical Engineering 2021: Enhancing Innovations and Applications of Chemical Engineering for Accelerating Sustainable Development Goals, ISIChem 2021
Y2 - 6 October 2021 through 7 October 2021
ER -