Influence of CTAB and sonication on nickel hydroxide nanoparticles synthesis by electrolysis at high voltage

Yanatra Budipramana, Suprapto, Taslim Ersam, Fredy Kurniawan*

*Corresponding author for this work

Research output: Chapter in Book/Report/Conference proceedingConference contributionpeer-review

4 Citations (Scopus)

Abstract

CTAB and Sonication has been used for preparing Ni(OH)2nanoparticles by electrolysis at high voltage. The effect of CTAB and sonication on the morphology and size of Ni(OH)2nanoparticles was observed. The results obtained were characterized with UV-Vis spectroscopy, X-ray Diffraction (XRD), Fourier Transform Infrared Spectrometer (FTIR), and Transmission Electron Microscopy (TEM). The TEM image shows that Ni(OH)2nanoparticles obtained with and without CTAB under sonication were nearly spherical. UV-Vis Spectrums show that with CTAB has higher concentration in comparison with without CTAB. But no significant different was found for FTIR spectrum. Thermogram shows Ni(OH)2nanoparticles obtained with and without CTAB have different properties at 60-140 °C due to association of water and CTAB. The most stable Ni(OH)2nanoparticles were obtained by addition CTAB under sonication.

Original languageEnglish
Title of host publicationProceedings of 2nd International Conference on Electrical Systems, Technology and Information, ICESTI 2015
EditorsFelix Pasila, Yusak Tanoto, Resmana Lim, Murtiyanto Santoso, Nemuel Daniel Pah
PublisherSpringer Verlag
Pages345-351
Number of pages7
ISBN (Print)9789812879868
DOIs
Publication statusPublished - 2016
Event2nd International Conference on Electrical Systems, Technology and Information, ICESTI 2015 - Bali, Indonesia
Duration: 9 Sept 201512 Sept 2015

Publication series

NameLecture Notes in Electrical Engineering
Volume365
ISSN (Print)1876-1100
ISSN (Electronic)1876-1119

Conference

Conference2nd International Conference on Electrical Systems, Technology and Information, ICESTI 2015
Country/TerritoryIndonesia
CityBali
Period9/09/1512/09/15

Keywords

  • CTAB
  • Ni(OH)
  • Nickel
  • Sonochemistry

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