Isoamyl (E)-3-(3,4-Dimethoxyphenyl)acrylate

Egar Pamela; Lukman Atmaja; Mardi Santoso

doi:10.3390/M1708

Isoamyl (E)-3-(3,4-Dimethoxyphenyl)acrylate

Egar Pamela
, Lukman Atmaja
, Mardi Santoso^*

^*Corresponding author for this work

Institut Teknologi Sepuluh Nopember

Research output: Contribution to journal › Article › peer-review

Abstract

Isoamyl (E)-3-(3,4-dimethoxyphenyl)acrylate (1) was obtained from the 2-methyl-6-nitrobenzoic anhydride (MNBA)/4-dimethylaminopyridine (DMAP)-catalyzed reaction at room temperature for 190 min in dichloromethane with a yield of 95%. The structure of isoamyl (E)-3-(3,4-dimethoxyphenyl)acrylate (1) was elucidated using NMR, FTIR, and high-resolution mass spectrometry. In vitro sun protection factor evaluation exhibited a value of 37.10 ± 0.03 which indicates that isoamyl (E)-3-(3,4-dimethoxyphenyl)acrylate (1) is a sunscreen agent with high protection.

Original language	English
Article number	M1708
Journal	MolBank
Volume	2023
Issue number	3
DOIs	https://doi.org/10.3390/M1708
Publication status	Published - Sept 2023

Keywords

isoamyl (E)-3-(3,4-dimethoxyphenyl)acrylate
sun protection factor
synthesis

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10.3390/M1708

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title = "Isoamyl (E)-3-(3,4-Dimethoxyphenyl)acrylate",

abstract = "Isoamyl (E)-3-(3,4-dimethoxyphenyl)acrylate (1) was obtained from the 2-methyl-6-nitrobenzoic anhydride (MNBA)/4-dimethylaminopyridine (DMAP)-catalyzed reaction at room temperature for 190 min in dichloromethane with a yield of 95\%. The structure of isoamyl (E)-3-(3,4-dimethoxyphenyl)acrylate (1) was elucidated using NMR, FTIR, and high-resolution mass spectrometry. In vitro sun protection factor evaluation exhibited a value of 37.10 ± 0.03 which indicates that isoamyl (E)-3-(3,4-dimethoxyphenyl)acrylate (1) is a sunscreen agent with high protection.",

keywords = "isoamyl (E)-3-(3,4-dimethoxyphenyl)acrylate, sun protection factor, synthesis",

author = "Egar Pamela and Lukman Atmaja and Mardi Santoso",

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year = "2023",

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doi = "10.3390/M1708",

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volume = "2023",

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T1 - Isoamyl (E)-3-(3,4-Dimethoxyphenyl)acrylate

AU - Pamela, Egar

AU - Atmaja, Lukman

AU - Santoso, Mardi

PY - 2023/9

Y1 - 2023/9

N2 - Isoamyl (E)-3-(3,4-dimethoxyphenyl)acrylate (1) was obtained from the 2-methyl-6-nitrobenzoic anhydride (MNBA)/4-dimethylaminopyridine (DMAP)-catalyzed reaction at room temperature for 190 min in dichloromethane with a yield of 95%. The structure of isoamyl (E)-3-(3,4-dimethoxyphenyl)acrylate (1) was elucidated using NMR, FTIR, and high-resolution mass spectrometry. In vitro sun protection factor evaluation exhibited a value of 37.10 ± 0.03 which indicates that isoamyl (E)-3-(3,4-dimethoxyphenyl)acrylate (1) is a sunscreen agent with high protection.

AB - Isoamyl (E)-3-(3,4-dimethoxyphenyl)acrylate (1) was obtained from the 2-methyl-6-nitrobenzoic anhydride (MNBA)/4-dimethylaminopyridine (DMAP)-catalyzed reaction at room temperature for 190 min in dichloromethane with a yield of 95%. The structure of isoamyl (E)-3-(3,4-dimethoxyphenyl)acrylate (1) was elucidated using NMR, FTIR, and high-resolution mass spectrometry. In vitro sun protection factor evaluation exhibited a value of 37.10 ± 0.03 which indicates that isoamyl (E)-3-(3,4-dimethoxyphenyl)acrylate (1) is a sunscreen agent with high protection.

KW - isoamyl (E)-3-(3,4-dimethoxyphenyl)acrylate

KW - sun protection factor

KW - synthesis

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DO - 10.3390/M1708

M3 - Article

AN - SCOPUS:85172781431

SN - 1422-8599

VL - 2023

JO - MolBank

JF - MolBank

IS - 3

M1 - M1708

ER -

Isoamyl (E)-3-(3,4-Dimethoxyphenyl)acrylate

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