Ketoprofen-β-cyclodextrin inclusion complexes formation by supercritical process technology

Sumarno*, Rizki Rahim, Prida Novarita Trisanti

*Corresponding author for this work

Research output: Chapter in Book/Report/Conference proceedingConference contributionpeer-review

2 Citations (Scopus)

Abstract

Ketoprofen was a poorly soluble which anti-inflammatory, analgesic and antipyretic drug, solubility of which can be enchanced by form complexation with β-cyclodextrin. Besides that, the inclusion complex reduces the incidence of gastrointestinal side effect of drug. The aims of this research are to study the effect of H2O concentration in the supercritical carbondioxide and operation condition in the formation of ketoprofen-β-Cyclodextrin inclusion complex. This research was began by dissolved H2O in supercritical CO2 at 40°C and various saturation pressures. Then, dissolved H2O contacted with (1:5 w/w) ketoprofen-β-Cyclodextrin mixture at 50°C and various operation pressures. It called saturation process. Saturation was done for ±2 hours with agitation process and continued by decompression process. The products were characterized by drug Release, Differential Scanning Calorimetry (DCS) dan Scanning Electron Microscopy (SEM) analyses. The percentage from this work were 76,82%-89,99% for inclusion complexes. The percentage drug release of ketoprofen were 82,83%-88,36% on various inclusion pressure and various inclusion period.

Original languageEnglish
Title of host publicationInternational Seminar on Fundamental and Application of Chemical Engineering 2016, ISFAChE 2016
Subtitle of host publicationProceedings of the 3rd International Seminar on Fundamental and Application of Chemical Engineering 2016
Editors Widiyastuti, Fadlilatul Taufany, Siti Nurkhamidah
PublisherAmerican Institute of Physics Inc.
ISBN (Electronic)9780735415102
DOIs
Publication statusPublished - 24 May 2017
Event3rd International Seminar on Fundamental and Application of Chemical Engineering 2016, ISFAChE 2016 - East Java, Indonesia
Duration: 1 Nov 20162 Nov 2016

Publication series

NameAIP Conference Proceedings
Volume1840
ISSN (Print)0094-243X
ISSN (Electronic)1551-7616

Conference

Conference3rd International Seminar on Fundamental and Application of Chemical Engineering 2016, ISFAChE 2016
Country/TerritoryIndonesia
CityEast Java
Period1/11/162/11/16

Keywords

  • Carbon dioxide
  • Complex Inclusion
  • Cyclodextrin
  • Ketoprofen
  • Supercritical
  • water

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