TY - JOUR
T1 - Production of bone implant filaments from blue crab shells (Portunus pelagicus) in various synthesis conditions and blending ratios of hydroxyapatite (HAp)-polycaprolactone (PCL)
AU - Ningrum, E. O.
AU - Pratiwi, E. L.
AU - Shaffitri, I. L.
AU - Putra, A. F.P.
AU - Karisma, A. D.
AU - Suprapto, S.
N1 - Publisher Copyright:
© 2022 Institute of Physics Publishing. All rights reserved.
PY - 2022/1/19
Y1 - 2022/1/19
N2 - The effect of calcination temperatures and KH2PO4 concentrations on filament properties using the precipitation method was investigated. Moreover, the effect of optimum hydroxyapatite-polycaprolactone ratios was also elucidated. In this study, blue crab shells (Portunus pelagicus) waste was used to synthesis hydroxyapatite. The modification of composite production was done by adding polymer as filler to obtain stronger composites with suitable mechanical properties for a stronger bone implant. The filament production consists of several steps, i.e., raw material pretreatment, synthesis of hydroxyapatite using a precursor of KH2PO4 with precipitation method, and synthesis of hydroxyapatite-polycaprolactone composites, and hydroxyapatite-polycaprolactone filament formation process using an extruder. It was found that the hydroxyapatite has been successfully synthesized from raw material of blue crab (Portunus Pelagicus) shells by calcination temperatures of 950°C and 1000°C. The highest calcium concentration in the raw material calcined from rajungan shells obtained from the XRF analysis was 94.96% at a temperature of 950°C. The FTIR analysis results showed a PO43- group indicating hydroxyapatite content in the crab shells.
AB - The effect of calcination temperatures and KH2PO4 concentrations on filament properties using the precipitation method was investigated. Moreover, the effect of optimum hydroxyapatite-polycaprolactone ratios was also elucidated. In this study, blue crab shells (Portunus pelagicus) waste was used to synthesis hydroxyapatite. The modification of composite production was done by adding polymer as filler to obtain stronger composites with suitable mechanical properties for a stronger bone implant. The filament production consists of several steps, i.e., raw material pretreatment, synthesis of hydroxyapatite using a precursor of KH2PO4 with precipitation method, and synthesis of hydroxyapatite-polycaprolactone composites, and hydroxyapatite-polycaprolactone filament formation process using an extruder. It was found that the hydroxyapatite has been successfully synthesized from raw material of blue crab (Portunus Pelagicus) shells by calcination temperatures of 950°C and 1000°C. The highest calcium concentration in the raw material calcined from rajungan shells obtained from the XRF analysis was 94.96% at a temperature of 950°C. The FTIR analysis results showed a PO43- group indicating hydroxyapatite content in the crab shells.
UR - http://www.scopus.com/inward/record.url?scp=85124106754&partnerID=8YFLogxK
U2 - 10.1088/1755-1315/963/1/012021
DO - 10.1088/1755-1315/963/1/012021
M3 - Conference article
AN - SCOPUS:85124106754
SN - 1755-1307
VL - 963
JO - IOP Conference Series: Earth and Environmental Science
JF - IOP Conference Series: Earth and Environmental Science
IS - 1
M1 - 012021
T2 - 2021 International Bioprocessing Association Subject Conference, IBASC 2021
Y2 - 4 August 2021 through 5 August 2021
ER -