Synthesis and characterization of Cu doped magnesium hydroxide fluoride, Mg1-xCuxFOH

A. Sirojul Anam Izza Rosyadi; Irmina K. Murwani

doi:10.1063/1.4978097

Synthesis and characterization of Cu doped magnesium hydroxide fluoride, Mg_1-xCu_xFOH

A. Sirojul Anam Izza Rosyadi^*, Irmina K. Murwani

^*Corresponding author for this work

Institut Teknologi Sepuluh Nopember

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

Abstract

A series of Cu doped magnesium hydroxide fluoride, Mg_1-xCu_xFOH, were synthesized via sol-gel method followed by vacuum drying. The characterization of synthesized solids with XRD revealed the presence of an X-ray amorphous phase of the samples and appearance of some humps. FTIR spectra of solids synthesized showed a band at 3700 cm^-1 which is an isolated OH group, wide band at 3750-3000 cm^-1 supported by the peak at 1650 cm^-1 indicated the presence of absorbed water on the surface. Characteristic peaks for Mg-F and Mg-O vibrations were seen at 500-400 cm^-1 and 600-500 cm^-1 respectively.

Original language	English
Title of host publication	International Conference on Chemistry, Chemical Process and Engineering, IC3PE 2017
Editors	Is Fatimah, Gani Purwiandono
Publisher	American Institute of Physics Inc.
ISBN (Electronic)	9780735414914
DOIs	https://doi.org/10.1063/1.4978097
Publication status	Published - 17 Mar 2017
Event	International Conference on Chemistry, Chemical Process and Engineering, IC3PE 2017 - Yogyakarta, Indonesia Duration: 15 Nov 2016 → 16 Nov 2016

Publication series

Name	AIP Conference Proceedings
Volume	1823
ISSN (Print)	0094-243X
ISSN (Electronic)	1551-7616

Conference

Conference	International Conference on Chemistry, Chemical Process and Engineering, IC3PE 2017
Country/Territory	Indonesia
City	Yogyakarta
Period	15/11/16 → 16/11/16

Access to Document

10.1063/1.4978097

Cite this

Rosyadi, A. S. A. I., & Murwani, I. K. (2017). Synthesis and characterization of Cu doped magnesium hydroxide fluoride, Mg_1-xCu_xFOH. In I. Fatimah, & G. Purwiandono (Eds.), International Conference on Chemistry, Chemical Process and Engineering, IC3PE 2017 Article 020024 (AIP Conference Proceedings; Vol. 1823). American Institute of Physics Inc.. https://doi.org/10.1063/1.4978097

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title = "Synthesis and characterization of Cu doped magnesium hydroxide fluoride, Mg1-xCuxFOH",

abstract = "A series of Cu doped magnesium hydroxide fluoride, Mg1-xCuxFOH, were synthesized via sol-gel method followed by vacuum drying. The characterization of synthesized solids with XRD revealed the presence of an X-ray amorphous phase of the samples and appearance of some humps. FTIR spectra of solids synthesized showed a band at 3700 cm-1 which is an isolated OH group, wide band at 3750-3000 cm-1 supported by the peak at 1650 cm-1 indicated the presence of absorbed water on the surface. Characteristic peaks for Mg-F and Mg-O vibrations were seen at 500-400 cm-1 and 600-500 cm-1 respectively.",

author = "Rosyadi, {A. Sirojul Anam Izza} and Murwani, {Irmina K.}",

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Rosyadi, ASAI & Murwani, IK 2017, Synthesis and characterization of Cu doped magnesium hydroxide fluoride, Mg_1-xCu_xFOH. in I Fatimah & G Purwiandono (eds), International Conference on Chemistry, Chemical Process and Engineering, IC3PE 2017., 020024, AIP Conference Proceedings, vol. 1823, American Institute of Physics Inc., International Conference on Chemistry, Chemical Process and Engineering, IC3PE 2017, Yogyakarta, Indonesia, 15/11/16. https://doi.org/10.1063/1.4978097

Synthesis and characterization of Cu doped magnesium hydroxide fluoride, Mg_1-xCu_xFOH. / Rosyadi, A. Sirojul Anam Izza; Murwani, Irmina K.
International Conference on Chemistry, Chemical Process and Engineering, IC3PE 2017. ed. / Is Fatimah; Gani Purwiandono. American Institute of Physics Inc., 2017. 020024 (AIP Conference Proceedings; Vol. 1823).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

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N2 - A series of Cu doped magnesium hydroxide fluoride, Mg1-xCuxFOH, were synthesized via sol-gel method followed by vacuum drying. The characterization of synthesized solids with XRD revealed the presence of an X-ray amorphous phase of the samples and appearance of some humps. FTIR spectra of solids synthesized showed a band at 3700 cm-1 which is an isolated OH group, wide band at 3750-3000 cm-1 supported by the peak at 1650 cm-1 indicated the presence of absorbed water on the surface. Characteristic peaks for Mg-F and Mg-O vibrations were seen at 500-400 cm-1 and 600-500 cm-1 respectively.

AB - A series of Cu doped magnesium hydroxide fluoride, Mg1-xCuxFOH, were synthesized via sol-gel method followed by vacuum drying. The characterization of synthesized solids with XRD revealed the presence of an X-ray amorphous phase of the samples and appearance of some humps. FTIR spectra of solids synthesized showed a band at 3700 cm-1 which is an isolated OH group, wide band at 3750-3000 cm-1 supported by the peak at 1650 cm-1 indicated the presence of absorbed water on the surface. Characteristic peaks for Mg-F and Mg-O vibrations were seen at 500-400 cm-1 and 600-500 cm-1 respectively.

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