Synthesis and characterization of Ni0.8Zn0.2Fe2O4nanoparticles by self combustion technique

Puspitasari Poppy; Azliza Ahmad Nur; Risdanareni Puput; Januarti Jaya Ekaputri

doi:10.4028/www.scientific.net/MSF.857.136

Synthesis and characterization of Ni_0.8Zn_0.2Fe₂O₄nanoparticles by self combustion technique

Puspitasari Poppy, Azliza Ahmad Nur, Risdanareni Puput, Januarti Jaya Ekaputri

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

Abstract

Nickel zinc ferrite (Ni_0.8Zn_0.2Fe₂O₄) is a soft ferrite material and can be use in electromagnetic applications that require a high permeability, such as electromagnetic wave absorbers. However synthesizing nanosize Ni_0.8Zn_0.2Fe₂O₄remains a challenge. This work deals with preparation of Ni_0.8Z_n0.2Fe₂O₄nanoparticles by using self combustion technique. The mixtures were annealed at 800 ◦C, 900 ◦C and 1200 ◦C. Characterizations were done by using X-Ray Diffractions (XRD), Raman Spectra, Field Emission Scanning Electron Microscope (FESEM) and Transmission Electron Microscope (TEM). The XRD patterns showed a major peak of [311] plane of the spinel cubic structure for Ni_0.8Zn_0.2Fe₂O₄samples. The average crystallites size are 20- 50 nm. Raman Spectra patterns had shown two major peaks located in the range located at in the range of 400- 700 cm^-1. FESEM morphology shown hexagon shape with average dimensions of 40-140 nm. From TEM morphologies, dimension of d-spacing are 2 nm and obtain the hexagon shape of Ni_0.8Zn_0.2Fe₂O₄. As a conclusion, the best morphology of Ni0.8Zn0.2Fe2O4 was obtained at temperature of 900 ◦C.

Original language	English
Title of host publication	Advanced Materials Engineering and Technology IV
Editors	Mohd Mustafa Al Bakri Abdullah, Rafiza Abd Razak, Muhammad Faheem Mohd Tahir, Mohd Mustafa Al Bakri Abdullah, Rafiza Abd Razak, Liyana Jamaludin
Publisher	Trans Tech Publications Ltd
Pages	136-141
Number of pages	6
ISBN (Print)	9783035710205
DOIs	https://doi.org/10.4028/www.scientific.net/MSF.857.136
Publication status	Published - 2016
Event	International Conference on Advanced Materials Engineering and Technology, ICAMET 2015 - Kaohsiung, Taiwan, Province of China Duration: 4 Dec 2015 → 5 Dec 2015

Publication series

Name	Materials Science Forum
Volume	857
ISSN (Print)	0255-5476
ISSN (Electronic)	1662-9752

Conference

Conference	International Conference on Advanced Materials Engineering and Technology, ICAMET 2015
Country/Territory	Taiwan, Province of China
City	Kaohsiung
Period	4/12/15 → 5/12/15

Keywords

Hexagon shape
Nickel zinc ferrites
Self-combustion technique

Access to Document

10.4028/www.scientific.net/MSF.857.136

Cite this

Poppy, P., Nur, A. A., Puput, R., & Ekaputri, J. J. (2016). Synthesis and characterization of Ni_0.8Zn_0.2Fe₂O₄nanoparticles by self combustion technique. In M. M. Al Bakri Abdullah, R. A. Razak, M. F. M. Tahir, M. M. Al Bakri Abdullah, R. A. Razak, & L. Jamaludin (Eds.), Advanced Materials Engineering and Technology IV (pp. 136-141). (Materials Science Forum; Vol. 857). Trans Tech Publications Ltd. https://doi.org/10.4028/www.scientific.net/MSF.857.136

Poppy, Puspitasari ; Nur, Azliza Ahmad ; Puput, Risdanareni et al. / Synthesis and characterization of Ni_0.8Zn_0.2Fe₂O₄nanoparticles by self combustion technique. Advanced Materials Engineering and Technology IV. editor / Mohd Mustafa Al Bakri Abdullah ; Rafiza Abd Razak ; Muhammad Faheem Mohd Tahir ; Mohd Mustafa Al Bakri Abdullah ; Rafiza Abd Razak ; Liyana Jamaludin. Trans Tech Publications Ltd, 2016. pp. 136-141 (Materials Science Forum).

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title = "Synthesis and characterization of Ni0.8Zn0.2Fe2O4nanoparticles by self combustion technique",

abstract = "Nickel zinc ferrite (Ni0.8Zn0.2Fe2O4) is a soft ferrite material and can be use in electromagnetic applications that require a high permeability, such as electromagnetic wave absorbers. However synthesizing nanosize Ni0.8Zn0.2Fe2O4remains a challenge. This work deals with preparation of Ni0.8Zn0.2Fe2O4nanoparticles by using self combustion technique. The mixtures were annealed at 800 ◦C, 900 ◦C and 1200 ◦C. Characterizations were done by using X-Ray Diffractions (XRD), Raman Spectra, Field Emission Scanning Electron Microscope (FESEM) and Transmission Electron Microscope (TEM). The XRD patterns showed a major peak of [311] plane of the spinel cubic structure for Ni0.8Zn0.2Fe2O4samples. The average crystallites size are 20- 50 nm. Raman Spectra patterns had shown two major peaks located in the range located at in the range of 400- 700 cm-1. FESEM morphology shown hexagon shape with average dimensions of 40-140 nm. From TEM morphologies, dimension of d-spacing are 2 nm and obtain the hexagon shape of Ni0.8Zn0.2Fe2O4. As a conclusion, the best morphology of Ni0.8Zn0.2Fe2O4 was obtained at temperature of 900 ◦C.",

keywords = "Hexagon shape, Nickel zinc ferrites, Self-combustion technique",

author = "Puspitasari Poppy and Nur, {Azliza Ahmad} and Risdanareni Puput and Ekaputri, {Januarti Jaya}",

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Poppy, P, Nur, AA, Puput, R & Ekaputri, JJ 2016, Synthesis and characterization of Ni_0.8Zn_0.2Fe₂O₄nanoparticles by self combustion technique. in MM Al Bakri Abdullah, RA Razak, MFM Tahir, MM Al Bakri Abdullah, RA Razak & L Jamaludin (eds), Advanced Materials Engineering and Technology IV. Materials Science Forum, vol. 857, Trans Tech Publications Ltd, pp. 136-141, International Conference on Advanced Materials Engineering and Technology, ICAMET 2015, Kaohsiung, Taiwan, Province of China, 4/12/15. https://doi.org/10.4028/www.scientific.net/MSF.857.136

Synthesis and characterization of Ni_0.8Zn_0.2Fe₂O₄nanoparticles by self combustion technique. / Poppy, Puspitasari; Nur, Azliza Ahmad; Puput, Risdanareni et al.
Advanced Materials Engineering and Technology IV. ed. / Mohd Mustafa Al Bakri Abdullah; Rafiza Abd Razak; Muhammad Faheem Mohd Tahir; Mohd Mustafa Al Bakri Abdullah; Rafiza Abd Razak; Liyana Jamaludin. Trans Tech Publications Ltd, 2016. p. 136-141 (Materials Science Forum; Vol. 857).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

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AU - Ekaputri, Januarti Jaya

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N2 - Nickel zinc ferrite (Ni0.8Zn0.2Fe2O4) is a soft ferrite material and can be use in electromagnetic applications that require a high permeability, such as electromagnetic wave absorbers. However synthesizing nanosize Ni0.8Zn0.2Fe2O4remains a challenge. This work deals with preparation of Ni0.8Zn0.2Fe2O4nanoparticles by using self combustion technique. The mixtures were annealed at 800 ◦C, 900 ◦C and 1200 ◦C. Characterizations were done by using X-Ray Diffractions (XRD), Raman Spectra, Field Emission Scanning Electron Microscope (FESEM) and Transmission Electron Microscope (TEM). The XRD patterns showed a major peak of [311] plane of the spinel cubic structure for Ni0.8Zn0.2Fe2O4samples. The average crystallites size are 20- 50 nm. Raman Spectra patterns had shown two major peaks located in the range located at in the range of 400- 700 cm-1. FESEM morphology shown hexagon shape with average dimensions of 40-140 nm. From TEM morphologies, dimension of d-spacing are 2 nm and obtain the hexagon shape of Ni0.8Zn0.2Fe2O4. As a conclusion, the best morphology of Ni0.8Zn0.2Fe2O4 was obtained at temperature of 900 ◦C.

AB - Nickel zinc ferrite (Ni0.8Zn0.2Fe2O4) is a soft ferrite material and can be use in electromagnetic applications that require a high permeability, such as electromagnetic wave absorbers. However synthesizing nanosize Ni0.8Zn0.2Fe2O4remains a challenge. This work deals with preparation of Ni0.8Zn0.2Fe2O4nanoparticles by using self combustion technique. The mixtures were annealed at 800 ◦C, 900 ◦C and 1200 ◦C. Characterizations were done by using X-Ray Diffractions (XRD), Raman Spectra, Field Emission Scanning Electron Microscope (FESEM) and Transmission Electron Microscope (TEM). The XRD patterns showed a major peak of [311] plane of the spinel cubic structure for Ni0.8Zn0.2Fe2O4samples. The average crystallites size are 20- 50 nm. Raman Spectra patterns had shown two major peaks located in the range located at in the range of 400- 700 cm-1. FESEM morphology shown hexagon shape with average dimensions of 40-140 nm. From TEM morphologies, dimension of d-spacing are 2 nm and obtain the hexagon shape of Ni0.8Zn0.2Fe2O4. As a conclusion, the best morphology of Ni0.8Zn0.2Fe2O4 was obtained at temperature of 900 ◦C.

KW - Hexagon shape

KW - Nickel zinc ferrites

KW - Self-combustion technique

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Poppy P, Nur AA, Puput R, Ekaputri JJ. Synthesis and characterization of Ni_0.8Zn_0.2Fe₂O₄nanoparticles by self combustion technique. In Al Bakri Abdullah MM, Razak RA, Tahir MFM, Al Bakri Abdullah MM, Razak RA, Jamaludin L, editors, Advanced Materials Engineering and Technology IV. Trans Tech Publications Ltd. 2016. p. 136-141. (Materials Science Forum). doi: 10.4028/www.scientific.net/MSF.857.136