Synthesis and toxicity test of tin(IV) pyridine-2,6-dicarboxylate complexes

Imanuel Gauru; Fahimah Martak

doi:10.1063/5.0062237

Synthesis and toxicity test of tin(IV) pyridine-2,6-dicarboxylate complexes

Imanuel Gauru^*, Fahimah Martak

^*Corresponding author for this work

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

Abstract

Binuclear tin(IV) complex with pyridine-2,6-dicarboxylic ligand has been synthesized using reflux method. The colorless crystals with cubic shape were obtained. Elemental analysis of Tin(IV) Pyridine-2,6-Dicarboxylate Complexes clearly indicates that the contents of carbon, hydrogen, and nitrogen in the complex were 31,74%, 3.08%, 4.23% by weight. The measurement of tin levels in the complexes by Atomic Absorption Spectroscopy (AAS) shows the results of 34.80% by weight. The IR spectrum showed absorption peaks of Sn-N and Sn=O at 432.05 and 732.95 cm-1 respectively, confirming the formation of complex. Toxicity of the complex was determined by Brine Shrimp Lethality Test (BSLT) method, and the LC50 value of the complex was 23.81 mg/L.

Original language	English
Title of host publication	3rd International Conference on Chemistry, Chemical Process and Engineering, IC3PE 2020
Editors	Is Fatimah, Won-Chun Oh, Imam Sahroni
Publisher	American Institute of Physics Inc.
ISBN (Electronic)	9780735441262
DOIs	https://doi.org/10.1063/5.0062237
Publication status	Published - 1 Sept 2021
Event	3rd International Conference on Chemistry, Chemical Process and Engineering, IC3PE 2020 - Yogyakarta, Indonesia Duration: 30 Sept 2020 → …

Publication series

Name	AIP Conference Proceedings
Volume	2370
ISSN (Print)	0094-243X
ISSN (Electronic)	1551-7616

Conference

Conference	3rd International Conference on Chemistry, Chemical Process and Engineering, IC3PE 2020
Country/Territory	Indonesia
City	Yogyakarta
Period	30/09/20 → …

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10.1063/5.0062237

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title = "Synthesis and toxicity test of tin(IV) pyridine-2,6-dicarboxylate complexes",

abstract = "Binuclear tin(IV) complex with pyridine-2,6-dicarboxylic ligand has been synthesized using reflux method. The colorless crystals with cubic shape were obtained. Elemental analysis of Tin(IV) Pyridine-2,6-Dicarboxylate Complexes clearly indicates that the contents of carbon, hydrogen, and nitrogen in the complex were 31,74%, 3.08%, 4.23% by weight. The measurement of tin levels in the complexes by Atomic Absorption Spectroscopy (AAS) shows the results of 34.80% by weight. The IR spectrum showed absorption peaks of Sn-N and Sn=O at 432.05 and 732.95 cm-1 respectively, confirming the formation of complex. Toxicity of the complex was determined by Brine Shrimp Lethality Test (BSLT) method, and the LC50 value of the complex was 23.81 mg/L.",

author = "Imanuel Gauru and Fahimah Martak",

note = "Publisher Copyright: {\textcopyright} 2021 Author(s).; 3rd International Conference on Chemistry, Chemical Process and Engineering, IC3PE 2020 ; Conference date: 30-09-2020",

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language = "English",

series = "AIP Conference Proceedings",

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Gauru, I & Martak, F 2021, Synthesis and toxicity test of tin(IV) pyridine-2,6-dicarboxylate complexes. in I Fatimah, W-C Oh & I Sahroni (eds), 3rd International Conference on Chemistry, Chemical Process and Engineering, IC3PE 2020., 020006, AIP Conference Proceedings, vol. 2370, American Institute of Physics Inc., 3rd International Conference on Chemistry, Chemical Process and Engineering, IC3PE 2020, Yogyakarta, Indonesia, 30/09/20. https://doi.org/10.1063/5.0062237

Synthesis and toxicity test of tin(IV) pyridine-2,6-dicarboxylate complexes. / Gauru, Imanuel; Martak, Fahimah.
3rd International Conference on Chemistry, Chemical Process and Engineering, IC3PE 2020. ed. / Is Fatimah; Won-Chun Oh; Imam Sahroni. American Institute of Physics Inc., 2021. 020006 (AIP Conference Proceedings; Vol. 2370).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

TY - GEN

T1 - Synthesis and toxicity test of tin(IV) pyridine-2,6-dicarboxylate complexes

AU - Gauru, Imanuel

AU - Martak, Fahimah

PY - 2021/9/1

Y1 - 2021/9/1

N2 - Binuclear tin(IV) complex with pyridine-2,6-dicarboxylic ligand has been synthesized using reflux method. The colorless crystals with cubic shape were obtained. Elemental analysis of Tin(IV) Pyridine-2,6-Dicarboxylate Complexes clearly indicates that the contents of carbon, hydrogen, and nitrogen in the complex were 31,74%, 3.08%, 4.23% by weight. The measurement of tin levels in the complexes by Atomic Absorption Spectroscopy (AAS) shows the results of 34.80% by weight. The IR spectrum showed absorption peaks of Sn-N and Sn=O at 432.05 and 732.95 cm-1 respectively, confirming the formation of complex. Toxicity of the complex was determined by Brine Shrimp Lethality Test (BSLT) method, and the LC50 value of the complex was 23.81 mg/L.

AB - Binuclear tin(IV) complex with pyridine-2,6-dicarboxylic ligand has been synthesized using reflux method. The colorless crystals with cubic shape were obtained. Elemental analysis of Tin(IV) Pyridine-2,6-Dicarboxylate Complexes clearly indicates that the contents of carbon, hydrogen, and nitrogen in the complex were 31,74%, 3.08%, 4.23% by weight. The measurement of tin levels in the complexes by Atomic Absorption Spectroscopy (AAS) shows the results of 34.80% by weight. The IR spectrum showed absorption peaks of Sn-N and Sn=O at 432.05 and 732.95 cm-1 respectively, confirming the formation of complex. Toxicity of the complex was determined by Brine Shrimp Lethality Test (BSLT) method, and the LC50 value of the complex was 23.81 mg/L.

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U2 - 10.1063/5.0062237

DO - 10.1063/5.0062237

M3 - Conference contribution

AN - SCOPUS:85114993337

T3 - AIP Conference Proceedings

BT - 3rd International Conference on Chemistry, Chemical Process and Engineering, IC3PE 2020

A2 - Fatimah, Is

A2 - Oh, Won-Chun

A2 - Sahroni, Imam

PB - American Institute of Physics Inc.

T2 - 3rd International Conference on Chemistry, Chemical Process and Engineering, IC3PE 2020

Y2 - 30 September 2020

ER -

Synthesis and toxicity test of tin(IV) pyridine-2,6-dicarboxylate complexes

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