TY - JOUR
T1 - Synthesis, Investigation on Structural and Magnetic Behaviors of Spinel M-Ferrite [M = Fe; Zn; Mn] Nanoparticles from Iron Sand
AU - Bahtiar, S.
AU - Taufiq, A.
AU - Sunaryono,
AU - Hidayat, A.
AU - Hidayat, N.
AU - Diantoro, M.
AU - Mufti, N.
AU - Mujamilah,
N1 - Publisher Copyright:
© Published under licence by IOP Publishing Ltd.
PY - 2017/5/31
Y1 - 2017/5/31
N2 - Spinel M-ferrite [M = Fe; Zn; Mn] nanoparticles were prepared from iron sand using a coprecipitation-sonochemical approach. The purified Fe3O4 from iron sand, ZnCl2 and MnCl2.4H2O, HCl, and NH4OH were used as raw materials. X-Ray Diffractometer (XRD), Fourier Transform Infra-Red (FTIR) spectroscopy, Transmission Electron Microscopy (TEM), and Vibration Sample Magnetometer (VSM) were employed to characterize the crystal structure, functional groups, particle size, morphology, and magnetic behavior of the prepared samples, respectively. From the XRD data analysis, M-ferrite particles exhibited a single phase in spinel structure. Furthermore, the M-ferrite particle increased their lattice parameter and crystal volume tracking the metallic-ionic radii of M. The particle size of the M-ferrites particles varied with M, whereas the biggest and lowest were for Zn and Mn, respectively. Based on the magnetization curve, the M-ferrite nanoparticles tended to perform a superparamagnetic behavior and their saturation magnetization as a function of their M ion and particle size.
AB - Spinel M-ferrite [M = Fe; Zn; Mn] nanoparticles were prepared from iron sand using a coprecipitation-sonochemical approach. The purified Fe3O4 from iron sand, ZnCl2 and MnCl2.4H2O, HCl, and NH4OH were used as raw materials. X-Ray Diffractometer (XRD), Fourier Transform Infra-Red (FTIR) spectroscopy, Transmission Electron Microscopy (TEM), and Vibration Sample Magnetometer (VSM) were employed to characterize the crystal structure, functional groups, particle size, morphology, and magnetic behavior of the prepared samples, respectively. From the XRD data analysis, M-ferrite particles exhibited a single phase in spinel structure. Furthermore, the M-ferrite particle increased their lattice parameter and crystal volume tracking the metallic-ionic radii of M. The particle size of the M-ferrites particles varied with M, whereas the biggest and lowest were for Zn and Mn, respectively. Based on the magnetization curve, the M-ferrite nanoparticles tended to perform a superparamagnetic behavior and their saturation magnetization as a function of their M ion and particle size.
KW - M-ferrite [M = Fe; Zn; Mn]
KW - coprecipitation
KW - magnetization
KW - nanoparticle
KW - sonochemical
KW - structure
UR - http://www.scopus.com/inward/record.url?scp=85021774781&partnerID=8YFLogxK
U2 - 10.1088/1757-899X/202/1/012052
DO - 10.1088/1757-899X/202/1/012052
M3 - Conference article
AN - SCOPUS:85021774781
SN - 1757-8981
VL - 202
JO - IOP Conference Series: Materials Science and Engineering
JF - IOP Conference Series: Materials Science and Engineering
IS - 1
M1 - 012052
T2 - 4th International Conference on Advanced Materials Science and Technology 2016, ICAMST 2016
Y2 - 27 September 2016 through 28 September 2016
ER -