The effect of CO2 gas flow rate on precipitated CaCO3 formed at room temperature

Fatimatul Munawaroh; Laila Khamsatul Muharrami; T. Triwikantoro; Zaenal Arifin

doi:10.1063/1.5054513

The effect of CO₂ gas flow rate on precipitated CaCO₃ formed at room temperature

Fatimatul Munawaroh^*, Laila Khamsatul Muharrami, T. Triwikantoro, Zaenal Arifin

^*Corresponding author for this work

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

5 Citations (Scopus)

Abstract

Synthesis of precipitated CaCO₃ from limestone Blumbungan, Madura island (East Java, Indonesia) using carbonation process have been done. The carbonation process is carried out with variations of the CO₂ gas flow rate of 1.175, 2.35, 3.525 and 4.7 l/min at room temperature. The crystalline phase formed was characterized by X-ray diffraction (XRD) X-Pert MPD with Cu-K_α radiation (λ = 1,5406) and scanned from 10°to 60°. The morphological investigation was analyzed by Scanning Electron microscope (SEM) FEI Inspect S50 X'pertPRO PANalytical. Crystal size was analyzed using the Scherrer equation. The XRD test results show that the phases formed at CO₂ gas flow rates 1.175, 2.35, and 3.525 l/min are vaterite and calcite, while at 4.7l/min only calcite phase is formed. Variations in CO₂ gas flow rate affect the percentage of calcite and vaterite formed. The crystal size of precipitated CaCO₃ the Scherrer equation ranged from 55,572 - 81,290 nm. The morphology of precipitated CaCO³ is mix rhombohedral cubic and needle-like.

Original language	English
Title of host publication	International Conference on Science and Applied Science, ICSAS 2018
Editors	M.A. Suparmi, Dewanta Arya Nugraha
Publisher	American Institute of Physics Inc.
ISBN (Print)	9780735417304
DOIs	https://doi.org/10.1063/1.5054513
Publication status	Published - 21 Sept 2018
Event	International Conference on Science and Applied Science, ICSAS 2018 - Surakarta, Indonesia Duration: 12 May 2018 → …

Publication series

Name	AIP Conference Proceedings
Volume	2014
ISSN (Print)	0094-243X
ISSN (Electronic)	1551-7616

Conference

Conference	International Conference on Science and Applied Science, ICSAS 2018
Country/Territory	Indonesia
City	Surakarta
Period	12/05/18 → …

Access to Document

10.1063/1.5054513

Cite this

Munawaroh, F., Muharrami, L. K., Triwikantoro, T., & Arifin, Z. (2018). The effect of CO₂ gas flow rate on precipitated CaCO₃ formed at room temperature. In M. A. Suparmi, & D. A. Nugraha (Eds.), International Conference on Science and Applied Science, ICSAS 2018 Article 020109 (AIP Conference Proceedings; Vol. 2014). American Institute of Physics Inc.. https://doi.org/10.1063/1.5054513

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title = "The effect of CO2 gas flow rate on precipitated CaCO3 formed at room temperature",

abstract = "Synthesis of precipitated CaCO3 from limestone Blumbungan, Madura island (East Java, Indonesia) using carbonation process have been done. The carbonation process is carried out with variations of the CO2 gas flow rate of 1.175, 2.35, 3.525 and 4.7 l/min at room temperature. The crystalline phase formed was characterized by X-ray diffraction (XRD) X-Pert MPD with Cu-Kα radiation (λ = 1,5406) and scanned from 10°to 60°. The morphological investigation was analyzed by Scanning Electron microscope (SEM) FEI Inspect S50 X'pertPRO PANalytical. Crystal size was analyzed using the Scherrer equation. The XRD test results show that the phases formed at CO2 gas flow rates 1.175, 2.35, and 3.525 l/min are vaterite and calcite, while at 4.7l/min only calcite phase is formed. Variations in CO2 gas flow rate affect the percentage of calcite and vaterite formed. The crystal size of precipitated CaCO3 the Scherrer equation ranged from 55,572 - 81,290 nm. The morphology of precipitated CaCO3 is mix rhombohedral cubic and needle-like.",

author = "Fatimatul Munawaroh and Muharrami, {Laila Khamsatul} and T. Triwikantoro and Zaenal Arifin",

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Munawaroh, F, Muharrami, LK, Triwikantoro, T & Arifin, Z 2018, The effect of CO₂ gas flow rate on precipitated CaCO₃ formed at room temperature. in MA Suparmi & DA Nugraha (eds), International Conference on Science and Applied Science, ICSAS 2018., 020109, AIP Conference Proceedings, vol. 2014, American Institute of Physics Inc., International Conference on Science and Applied Science, ICSAS 2018, Surakarta, Indonesia, 12/05/18. https://doi.org/10.1063/1.5054513

The effect of CO₂ gas flow rate on precipitated CaCO₃ formed at room temperature. / Munawaroh, Fatimatul; Muharrami, Laila Khamsatul; Triwikantoro, T. et al.
International Conference on Science and Applied Science, ICSAS 2018. ed. / M.A. Suparmi; Dewanta Arya Nugraha. American Institute of Physics Inc., 2018. 020109 (AIP Conference Proceedings; Vol. 2014).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

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