Utilization of modified ZSM-5 as filler for polyethersulfone (PES) membrane

A. I. Rozafia; K. Roziqin; Y. L. Ni'Mah; W. P. Utomo; M. Zainuri; D. Hartanto

doi:10.1063/5.0001693

Utilization of modified ZSM-5 as filler for polyethersulfone (PES) membrane

A. I. Rozafia, K. Roziqin, Y. L. Ni'Mah, W. P. Utomo, M. Zainuri, D. Hartanto^*

^*Corresponding author for this work

Institut Teknologi Sepuluh Nopember

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

1 Citation (Scopus)

Abstract

The modified ZSM-5 commercial as a filler for the polyethersulfone membrane was investigated in this work. The modification of ZSM-5 was prepared from aqueous solution 0.25 M NaOH as long as 30 minutes and returned to H-ZSM-5 from by exchange with NH4-acetate and calcined at 550 °C. The ZSM-5 commercial and H-ZSM-5 were characterized by X-Ray Diffraction (XRD) and Fourier Transform Infrared Spectroscopy (FTIR). XRD analysis showed the presence of ZSM-5 and the desilication treatment did not have a significant effect on the structural crystal phase of ZSM-5. The FTIR analysis shows support for XRD data that the similarity of the peaks and absence of any new bonding formation after the desilication process, it has vibrations of the pentacle and Si-O, Al-O skeletons peaks in 545 and 450 cm^-1 which were characteristic of the ZSM-5. Modified ZSM-5 was as a filler in preparing the PES membrane by a phase inversion method. XRD data analysis shows that the composite membranes have characteristic peaks of ZSM-5 particle and amorphous PES and in the SEM image of cross section was seen as an asymmetrical membrane with tending a pore structure to be finger-like. The presence of ZSM-5 and PES in the composite membrane shows that ZSM-5 can be use as a filler in PES membranes.

Original language	English
Title of host publication	8th International Conference of the Indonesian Chemical Society, ICICS 2019
Editors	Mohamad Rafi, Rudi Heryanto, Wulan Tri Wahyuni
Publisher	American Institute of Physics Inc.
ISBN (Electronic)	9780735420021
DOIs	https://doi.org/10.1063/5.0001693
Publication status	Published - 4 Jun 2020
Event	8th International Conference of the Indonesian Chemical Society 2019, ICICS 2019 - Bogor, Indonesia Duration: 6 Aug 2019 → 7 Aug 2019

Publication series

Name	AIP Conference Proceedings
Volume	2243
ISSN (Print)	0094-243X
ISSN (Electronic)	1551-7616

Conference

Conference	8th International Conference of the Indonesian Chemical Society 2019, ICICS 2019
Country/Territory	Indonesia
City	Bogor
Period	6/08/19 → 7/08/19

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10.1063/5.0001693

Cite this

Rozafia, A. I., Roziqin, K., Ni'Mah, Y. L., Utomo, W. P., Zainuri, M., & Hartanto, D. (2020). Utilization of modified ZSM-5 as filler for polyethersulfone (PES) membrane. In M. Rafi, R. Heryanto, & W. T. Wahyuni (Eds.), 8th International Conference of the Indonesian Chemical Society, ICICS 2019 Article 030021 (AIP Conference Proceedings; Vol. 2243). American Institute of Physics Inc.. https://doi.org/10.1063/5.0001693

@inproceedings{2306e095c6e649a0aef7ab6cc41a84eb,

title = "Utilization of modified ZSM-5 as filler for polyethersulfone (PES) membrane",

abstract = "The modified ZSM-5 commercial as a filler for the polyethersulfone membrane was investigated in this work. The modification of ZSM-5 was prepared from aqueous solution 0.25 M NaOH as long as 30 minutes and returned to H-ZSM-5 from by exchange with NH4-acetate and calcined at 550 °C. The ZSM-5 commercial and H-ZSM-5 were characterized by X-Ray Diffraction (XRD) and Fourier Transform Infrared Spectroscopy (FTIR). XRD analysis showed the presence of ZSM-5 and the desilication treatment did not have a significant effect on the structural crystal phase of ZSM-5. The FTIR analysis shows support for XRD data that the similarity of the peaks and absence of any new bonding formation after the desilication process, it has vibrations of the pentacle and Si-O, Al-O skeletons peaks in 545 and 450 cm-1 which were characteristic of the ZSM-5. Modified ZSM-5 was as a filler in preparing the PES membrane by a phase inversion method. XRD data analysis shows that the composite membranes have characteristic peaks of ZSM-5 particle and amorphous PES and in the SEM image of cross section was seen as an asymmetrical membrane with tending a pore structure to be finger-like. The presence of ZSM-5 and PES in the composite membrane shows that ZSM-5 can be use as a filler in PES membranes.",

author = "Rozafia, {A. I.} and K. Roziqin and Ni'Mah, {Y. L.} and Utomo, {W. P.} and M. Zainuri and D. Hartanto",

note = "Publisher Copyright: {\textcopyright} 2020 Author(s).; 8th International Conference of the Indonesian Chemical Society 2019, ICICS 2019 ; Conference date: 06-08-2019 Through 07-08-2019",

year = "2020",

month = jun,

day = "4",

doi = "10.1063/5.0001693",

language = "English",

series = "AIP Conference Proceedings",

publisher = "American Institute of Physics Inc.",

editor = "Mohamad Rafi and Rudi Heryanto and Wahyuni, {Wulan Tri}",

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Rozafia, AI, Roziqin, K, Ni'Mah, YL , Utomo, WP , Zainuri, M & Hartanto, D 2020, Utilization of modified ZSM-5 as filler for polyethersulfone (PES) membrane. in M Rafi, R Heryanto & WT Wahyuni (eds), 8th International Conference of the Indonesian Chemical Society, ICICS 2019., 030021, AIP Conference Proceedings, vol. 2243, American Institute of Physics Inc., 8th International Conference of the Indonesian Chemical Society 2019, ICICS 2019, Bogor, Indonesia, 6/08/19. https://doi.org/10.1063/5.0001693

Utilization of modified ZSM-5 as filler for polyethersulfone (PES) membrane. / Rozafia, A. I.; Roziqin, K.; Ni'Mah, Y. L. et al.
8th International Conference of the Indonesian Chemical Society, ICICS 2019. ed. / Mohamad Rafi; Rudi Heryanto; Wulan Tri Wahyuni. American Institute of Physics Inc., 2020. 030021 (AIP Conference Proceedings; Vol. 2243).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

TY - GEN

T1 - Utilization of modified ZSM-5 as filler for polyethersulfone (PES) membrane

AU - Rozafia, A. I.

AU - Roziqin, K.

AU - Ni'Mah, Y. L.

AU - Utomo, W. P.

AU - Zainuri, M.

AU - Hartanto, D.

PY - 2020/6/4

Y1 - 2020/6/4

N2 - The modified ZSM-5 commercial as a filler for the polyethersulfone membrane was investigated in this work. The modification of ZSM-5 was prepared from aqueous solution 0.25 M NaOH as long as 30 minutes and returned to H-ZSM-5 from by exchange with NH4-acetate and calcined at 550 °C. The ZSM-5 commercial and H-ZSM-5 were characterized by X-Ray Diffraction (XRD) and Fourier Transform Infrared Spectroscopy (FTIR). XRD analysis showed the presence of ZSM-5 and the desilication treatment did not have a significant effect on the structural crystal phase of ZSM-5. The FTIR analysis shows support for XRD data that the similarity of the peaks and absence of any new bonding formation after the desilication process, it has vibrations of the pentacle and Si-O, Al-O skeletons peaks in 545 and 450 cm-1 which were characteristic of the ZSM-5. Modified ZSM-5 was as a filler in preparing the PES membrane by a phase inversion method. XRD data analysis shows that the composite membranes have characteristic peaks of ZSM-5 particle and amorphous PES and in the SEM image of cross section was seen as an asymmetrical membrane with tending a pore structure to be finger-like. The presence of ZSM-5 and PES in the composite membrane shows that ZSM-5 can be use as a filler in PES membranes.

AB - The modified ZSM-5 commercial as a filler for the polyethersulfone membrane was investigated in this work. The modification of ZSM-5 was prepared from aqueous solution 0.25 M NaOH as long as 30 minutes and returned to H-ZSM-5 from by exchange with NH4-acetate and calcined at 550 °C. The ZSM-5 commercial and H-ZSM-5 were characterized by X-Ray Diffraction (XRD) and Fourier Transform Infrared Spectroscopy (FTIR). XRD analysis showed the presence of ZSM-5 and the desilication treatment did not have a significant effect on the structural crystal phase of ZSM-5. The FTIR analysis shows support for XRD data that the similarity of the peaks and absence of any new bonding formation after the desilication process, it has vibrations of the pentacle and Si-O, Al-O skeletons peaks in 545 and 450 cm-1 which were characteristic of the ZSM-5. Modified ZSM-5 was as a filler in preparing the PES membrane by a phase inversion method. XRD data analysis shows that the composite membranes have characteristic peaks of ZSM-5 particle and amorphous PES and in the SEM image of cross section was seen as an asymmetrical membrane with tending a pore structure to be finger-like. The presence of ZSM-5 and PES in the composite membrane shows that ZSM-5 can be use as a filler in PES membranes.

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U2 - 10.1063/5.0001693

DO - 10.1063/5.0001693

M3 - Conference contribution

AN - SCOPUS:85086669855

T3 - AIP Conference Proceedings

BT - 8th International Conference of the Indonesian Chemical Society, ICICS 2019

A2 - Rafi, Mohamad

A2 - Heryanto, Rudi

A2 - Wahyuni, Wulan Tri

PB - American Institute of Physics Inc.

T2 - 8th International Conference of the Indonesian Chemical Society 2019, ICICS 2019

Y2 - 6 August 2019 through 7 August 2019

ER -

Utilization of modified ZSM-5 as filler for polyethersulfone (PES) membrane

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